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by | Mar 16, 2018 | Hosta

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Nitroapocynin is a mono-nitrated form of apocynin.

Synthesis

Apocynin can be nitrated with sodium nitrate and acidic ionic liquid 1-butyl-3-methylimidazolium hexafluorophosphate in acetonitrile solvent.[1][2]

References

  1. ^ Tajik, H.; Niknam, K.; Parsa, F. (2009). "Using acidic ionic liquid 1-butyl-3-methylimidazolium hydrogen sulfate in selective nitration of phenols under mild conditions". Journal of the Iranian Chemical Society. 6: 159–164. doi:10.1007/BF03246515. S2CID 55676239.
  2. ^ Babu, Sainath; Raghavamenon, Achuthan C.; Fronczek, Frank R.; Uppu, Rao M. (2009). "4-Hydroxy-3-methoxy-5-nitroacetophenone (5-nitroapocynin)". Acta Crystallographica Section E. 65 (9): o2292-3. doi:10.1107/S160053680903390X. PMC 2969931. PMID 21577684.
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